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El titulo alcohólico es igual al número de litros de alcohol etílico absoluto, contenidos en 100 litros de vino, medidos ambos volúmenes a la misma temperatura, y se expresan con una precisión de 0,1º % vol.
Se determina por destilación simple, del líquido neutralizado, y medida la densidad del destilado por areometría.
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1. Mídanse 250 mL de vino en el matraz aforado. Introduzca el vino en el matraz de destilación de 1 litro y enjuage con unos 10 mL de agua destilada el matraz de 250 mL y viértanlos en el matraz de destilación. Repita la operación unas 2 -3 veces.
2. Neutralize la muestra de vino a analizar con unos 10 mL de solución de Oxido de Calcio. Preparar la solución con mucha precaución a razón de 120 grs. de Calcio Oxido por litro de agua destilada.
3. Coloque el matraz de destilación encima del aro con la malla. Únalo con la columna rectificadora vigreux y ésta con el refrigerante serpentín mediante el doble codo. Sírvase del mismo matraz aforado como colector del destilado.
4. Coloque el mechero bunsen debajo del matraz y enciendalo. Verifique la destilación procurando que el agua del refrigerante esté siempre fría.
5. Proceder a la destilación hasta llenar el matraz de 250 mL a falta de unos 2 cm. del enrase. Apagar el mechero y retirar del destilador y enrasar con agua destilada.
6. Viértase el líquido destilado en la probeta de 250 mL, tápela y remuévala.
7. Mida la temperatura, luego sumérjase en el líquido un alcohómetro adecuado a la graduación que aprecie décimas de grado, y calibrarlo a 20 ºC, procurando que esté limpio y seco, y teniendo cuidado de acompañarlo hasta que flote. El alcohómetro debe tomarse por el extremo del vástago.
8. Cuando el alcohómetro esté en reposo sin que roce con las paredes de la probeta, y las burbujas de aire hayan desaparecido, se lee por debajo del menisco que forma el líquido.
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En el caso de destilar vinos que aún no han terminado la fermentación o no han sido filtrados o que contienen anhídrido carbónico en disolución, susceptibles de hacer espuma al entrar en ebullición y de penetrar aquella en el serpentín inutilizando la operación, se añadirá al vino, antes de destilar, algunas gotas de silicona antiespumante, cuyas substancias anulan la excesiva producción de espuma.
Consulte las tablas de corrección de temperatura en la sección Tablas à Correcciones Alcohométricas
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